水熱合成反應釜（HYDROTHERMAL AUTOCLAVE REACTOR） 水熱壓釜用于在高壓、高溫下進行水熱反應。水熱合成反應器通常有兩種類型;聚四氟

水熱合成反應釜（HYDROTHERMAL AUTOCLAVE REACTOR）

水熱壓釜用于在高壓、高溫下進行水熱反應。水熱合成反應器通常有兩種類型;聚四氟乙烯(PTFE)或聚四氟乙烯(TFM)內襯水熱壓釜反應器。（The Hydrothermal Autoclave reactor use to carry hydrothermal reaction at high pressure and high temperature. Hydrothermal synthesis reactor generally comes in a two variety; the Polytetrafluoroethylene (PTFE) or Teflon (TFM) lined hydrothermal autoclave reactors.）

水熱反應器主要由兩部分組成;外部優質不銹鋼護套和內部特氟龍內襯或特氟龍腔。在聚四氟乙烯內襯的高壓釜中，反應在最高240攝氏度下進行，而安全溫度是200攝氏度。（Hydrothermal reactor mainly made up of two parts; outer high-quality stainless steel jacket and inner Teflon liner or Teflon chamber. In the Teflon-lined autoclave, the reaction is carried out at maximum 240-degree Celsius, while the safe temperature is 200-degree Celsius. ）

操作指導（OPERATING GUIDE）

1. 1. 將高壓滅菌器和滅菌材料放在桌上或架子上。Place the Autoclave and sterilizing material on the table or on the shelf.

2. 逆時針擰擰螺紋型一級SS帽(SS合金304)，直到打開為止。Twist the screw type threaded primary SS cap (SS Alloy 304) in an anticlockwise direction until it has been opened.

3. 在反應器中有兩種類型的SS墊圈/蓋子，一種在底部，另一種在特氟隆容器腔的頂部。There is 2 type of SS gasket/lid in the reactor, 1 is on the bottom side and another is on top of the Teflon vessel chamber.

4. 提起頂部SS墊圈或蓋子，取出乳白色PTFE/Teflon反應室。Lift the top SS gasket or lid and take-out milky white color PTFE/Teflon reaction chamber.

5. 現在在反應室內填滿溶劑(根據襯墊的容量)并密封。Now fill solvent (as per liner's capacity) in the reaction chamber and sealed it.

6. 確保聚四氟乙烯蓋是氣密的，以避免壓力泄漏。Make sure that the Teflon cap should be air-tight to avoid pressure leakage.

7. 將聚四氟乙烯或聚四氟乙烯襯墊置于不銹鋼腔內。Place Teflon or PTFE liner in a stainless steel chamber.

8. 保持頂部墊圈在容器上方，并確保特氟綸內襯容器正確地放置在不銹鋼腔室中。Keep top gasket over the vessel and make sure that the Teflon-lined vessel placed properly in the Stainless Steel chamber.

9. 然后在順時針方向扭轉初級SS帽，直到它不再轉動。Then twist primary SS cap in a clockwise direction until it does not turn anymore.

10.在主帽的頂部安裝了二級SS帽，用于額外收緊，以避免壓力泄漏。The secondary SS cap has been given at the top of the primary cap for extra tightening to avoid pressure leakages.

11.在鎖定桿的幫助下，順時針方向旋轉一級不銹鋼帽，以進一步緊固。Rotate primary SS cap in the clockwise direction with the help of locking rod for additional tightening.

12.將水熱壓罐置于烘箱或爐內加熱至反應器安全溫度。Placed the hydrothermal autoclave in oven or furnace and heat it till reactor’s safe temperature.

13.增加烤箱的溫度，并設定加熱速度僅為5℃/分鐘。Increase the temperature of the oven and set heating rate 5 0C/minute only.

14.研究人員可以將水熱高壓釜加熱到200℃，以保證安全使用。A researcher can heat the hydrothermal autoclave till 200 0C for safe use.

15.水熱合成反應完成后，高壓釜的冷卻速度為5 0C/min。After completion of the hydrothermal synthesis reaction, the autoclave's cooling rate will be 5 0C/minute.

16.確保，在過程完成后，清潔PTFE或特氟龍襯墊適當地重復使用。Make sure that, after completion of the process clean PTFE or Teflon liner properly for reuse.

預防PRECAUTIONS

1. 不要在沒有水的情況下操作高壓釜。避免使用硬水。Do not operate the autoclave without water. Avoid using hard-water in the unit.

2. 使用聚四氟乙烯反應容器前應適當清潔，以避免污染。Clean Teflon reaction vessel properly before use to avoid contamination.

3. 不要在高壓釜上增加任何額外的重量。Do not put any extra weight on the autoclave.

4. 正確關閉蒸壓罐的蓋子，在沒有擰緊桿的幫助下先松開一級不銹鋼蓋子之前，不要試圖強行打開它。Close the autoclave caps properly, never try to open it by force without first loosening of primary SS cap with the help of tightening rod.

5. 水熱反應堆機組在一天的使用后進行清潔和干燥。Clean and Dry the hydrothermal reactor unit after a day uses.

6. 高壓釜僅用于其預定用途。Use Autoclave only for its intended purpose.

7. 確保壓力表工作正常。Ensure that the pressure gauge is operating correctly.

8. 確保兩個不銹鋼墊圈處于良好的形狀和狀態。Make sure the both stainless steel gaskets are in a good Shape & condition.

9. 清潔墊片所在的底座表面。Clean the surface of the base unit where gasket rests.

10.不要潤滑墊圈。Do not lubricate Gasket.